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Table 1 The MWCNT specimen treated under various H2/O2gas compositions; the characterization results of XPS; and theI D/I Gratio of Raman spectra

From: Effects of Gas Composition on Highly Efficient Surface Modification of Multi-Walled Carbon Nanotubes by Cation Treatment

Specimen (H2/O2(sccm/sccm))

XPS

Raman

sp 2(%)

sp 3(%)

–C–O (%)

–C=O (%)

–COO (%)

[O]/[C]a(%)

(I D /I G )

0/50

44.2

44.6

<0.1

9.4

1.7

11.1

1.03

10/40

40.5

39.5

11.9

0.8

7.3

20

1.05

25/25

42.8

26.1

13.8

17.3

<0.1

31.1

1.07

40/10

36.8

49.1

0.6

0.5

12.9

14

1.27

50/0

30.8

54

2.1

11

2.2

15.3

1.08

Pristine

48.8

40

1

8.4

1.8

11.2

0.89

  1. a[O]/[C]: the ratio of oxygenated groups to the total number of carbon atoms detected

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