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Table 1 Maximum diameter (Ø) of Sn droplets (DPs) and Sn x N y NWs obtained from heating up Sn under NH3and from the reaction of Sn + NH4Cl respectively, at different temperatures. In all cases a ramp rate of 30 °C/min was used to reachTGunder 250 sccm’s of NH3which was then maintained for a further 60 min at the growth temperature and after which the reactor was allowed to cool down to RT in a reduced flow of 50 sccm’s NH3

From: Synthesis of Tin Nitride Sn x N y Nanowires by Chemical Vapour Deposition

TG( °C)

Max Ø of Sn DPs (Sn:NH3)

Max Ø Sn x N y NWs (Sn + NH4Cl:NH3)

300

No DPs

No NWs

400

200 nm

200 nm

450

200 nm

500

500 nm

No NWs

600

500 nm

No NWs

700

2.0 μm

800

5.0 μm

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