Table 2 Polycondensation of OTSH and Zn(OAc) 2 under various conditions
Run | Temperature (°C) | Dioxane (L/molOTSH) | Yield (%)a | Mn(Mw/Mn)b | Rh(nm)c |
---|---|---|---|---|---|
1 | 40 | 25 | 31 | 5,800 (1.4) | 28 |
2 | 60 | 25 | 46 | 7,400 (1.4) | 82 |
3 | 80 | 25 | 43 | 7,700 (1.6) | 85 |
4 | 60 | 12.5 | 46 | 8,300 (2.1) | 83 |
5 | 60 | 37.5 | 42 | 7,000 (1.6) | 61 |