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Table 3 DMTA studies: temperatures of the relaxation processes

From: Relaxation processes in hybrid organic-inorganic polymer nanosystems polymerized in situ

Compositions

Relaxation temperatures (ω = 1 Hz)

Reactivity (R)

MDI (%)

PIC (%)

Tr0(°C)

Tr1(°C)

Tr2(°C)

0.04

100

0

−94

−43

-

0.06

90

10

−92

−42

-

0.1

80

20

−89

−39

56

0.14

65

35

−79

−39

64

0.16

58

42

−76

−43

67

0.18

50

50

−73

−46

76

0.22

35

65

−71

−52

82

0.26

20

80

−69

−74

86

  1. Compositions and glass transition temperatures of OIS obtained from DMTA investigations at frequency ω = 1 Hz, depending on the reactivity R of the organic component of OIS.

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