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Table 1 GPC and 1 H NMR data of (PCL) 2 (PDEA- b -PPEGMA) 2 polymers

From: pH-responsive micelles based on (PCL)2(PDEA-b-PPEGMA)2 miktoarm polymer: controlled synthesis, characterization, and application as anticancer drug carrier

Entry

Samplea

M n, GPC b

Mw/Mnb

M n, NMR c

M n, RealIR d

1

(PCL24)2(PDEA16-b-PPEGMA19)2

14,888

1.28

29,617

28,200

2

(PCL24)2(PDEA37-b-PPEGMA15)2

12,692

1.19

33,977

34,300

3

(PCL38)2(PDEA26-b-PPEGMA11)2

18,302

1.19

29,530

28,524

4

(PCL38)2(PDEA17-b-PPEGMA9)2

13,586

1.35

24,480

24,614

5

(PCL32)2(PDEA25-b-PPEGMA22)2

19,389

1.41

37,766

38,114

6

(PCL32)2(PDEA20-b-PPEGMA19)2

18,707

1.37

32,907

32,120

  1. aThe subscripts of PCL, PDEA and PPEGMA were the DP of PCL (x), PDEA (y) and PPEGMA (z) calculated from 1H NMR spectrum; bmeasured by GPC in THF; ccalculated by the equations Mn, NMR = (114 × x + 185 × y + 475 × z ) × 2 + 434; dcalculated by monomer conversion from the ReactIR.
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