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Table 1 Thermal analysis data for the thiomolybdates decomposition in N2

From: Low-Temperature Thermally Reduced Molybdenum Disulfide as a Pt-Free Counter Electrode for Dye-Sensitized Solar Cells

Compound

TG region

Temperature range (°C)

Probable product

Experimental weight loss (%)

(NH4)2MoS4

1

RT −200

MoS3

21.08

2

200–900

MoS2

45.50

(NH4)2MoS4 + DMF

1

RT −225

MoS3(+DMF)

24.51

2

225–900

MoS2

73.31

MoS2

1

RT −900

MoS2

<1

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