Table 1 Thermal analysis data for the thiomolybdates decomposition in N2
Compound | TG region | Temperature range (°C) | Probable product | Experimental weight loss (%) |
---|---|---|---|---|
(NH4)2MoS4 | 1 | RT −200 | MoS3 | 21.08 |
2 | 200–900 | MoS2 | 45.50 | |
(NH4)2MoS4 + DMF | 1 | RT −225 | MoS3(+DMF) | 24.51 |
2 | 225–900 | MoS2 | 73.31 | |
MoS2 | 1 | RT −900 | MoS2 | <1 |