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Table 1 Literature data and own experimental results concerning nominal compositions and observed phases in the produced Ni-Sn NPs together with temperature of synthesis

From: Synthesis and Characterization of Pure Ni and Ni-Sn Intermetallic Nanoparticles

Nominal ratio (mole fraction)

Synthesistemperature

Observed phases

Ref.

Ni

Sn

3

1

Room temperature

Ni3Sn2

  

[7]

6

1

Ni3Sn

  

2

1

Room temperature

Sn6O4(OH)4

Sn

 

[8]

1

1

Sn6O4(OH)4

Sn

 

2

3

NiSn

Ni3Sn

Sn

1

2

NiSn

Ni3Sn

Sn

19

1

Room temperature

unknown

[10]

6

1

Ni(OH)2

Ni3Sna

  

2

1

Nia

Sna

 

2

3

Sn(OH)2

Sna

  

3

1

Solution prepared at 323 K and refluxed at 470 K for 2.5 h

Ni3Sn

Ni3Sn2

 

[14]

3

2

Ni3Sn

Ni3Sn2

 

1

1

Ni3Sn

Ni3Sn2

 

3

1

 

Ni2.7Sn2

  

This paper

3

2

343 K

Ni2.7Sn2

Ni

 

3

4

 

Ni2.7Sn2

Ni

 

3

1

Solution prepared at 323 K and refluxed at 473 K for 0.5 h

Not indexed

This paper

3

2

Ni2.7Sn2

  

3

4

Ni2.7Sn2

  
  1. aAfterwards annealed under N2 atmosphere for 3 h at 773 K

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