Table 1 Detailed experimental conditions for synthesis of different types of metal sulfide NCs
From: A General One-Pot Approach to Synthesize Binary and Ternary Metal Sulfide Nanocrystals
Samples | Metal precursors | DDT | ODE | Temperature | Morphology |
|---|---|---|---|---|---|
PbS | 3 mmol Pb(OAc)2 xH2O | 20 mL | – | 200 °C | Octahedral |
Cu2S | 3 mmol Cu(acac)2 | 10 mL | 20 mL | 200 °C | Spherical |
ZnS | 3 mmol Zn(acac)2 | 5 mL | 25 mL | 240 °C | Shapeless |
CdS | 5 mmol Cd(acac)2 | 30 mL | – | 200 °C | Near-spherical |
Ag2S | 3 mmol Ag(OAc) | 20 mL | – | 205 °C | Spherical |
CdS:Cu(I) | 4.5 mmol Cd(acac)2 + 0.5 mmol Cu(acac)2 | 30 mL | – | 200 °C | Near-spherical |
CuInS2 | 3.1 mmol Cu(acac)2 + 1.9 mmol In(acac)3 | 5 mL | 25 mL | 240 °C | Bullet |