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Table 1 A set of parameters obtained for antibacterial activities of single zinc, iron, and manganese oxides

From: A Review on Enhancing the Antibacterial Activity of ZnO: Mechanisms and Microscopic Investigation

Method

Bacteria’s used

Precursors used

Morphological analysis

Highest ZI (mm)

Ref.

Zn

Other

SEM/TEM/HRTEM/SAED

Hydrothermal and calcination

S. aureus ATCC23235, B. subtilis ATCC23857, E. coli ATCC25922, B. pertussis ATCC9797, P.s aeruginosa Pao1ATCC15692

KMnO4, AlCl3.6H2O, and sodium dodecyl benzene sulfonates

20 nm mean diameter NRs

18 mm on P. aeruginosa

[9]

Green and precipitation

E. coli (ATCC 25922) and S. aureus

Mn(AC)2·4H2O

CTMAB and tea extract

Crystalline spherical and cubes NPs with 20–50 nm size

[10]

One-step sonochemical

S. aureus and E. coli

Zn(AC)2.2H2O

Dull appearance of PVA polymer with dispersed 4–6 nm ZnO NPs

[14]

Soft-solution

S. aureus (KCTC No. 3881) and K. pneumoniae(KCTC No. 2246)

Zn(AC)2.2H2O

ZnO NPs (0001): 60 nm × 10 nm spherical ZnO NAs: 10 nm

Conventional NPS: 30 nm

[16]

Ultrasonication and milling

E. coli (DH5α)

Commercial ZnO

ZnO nanofluid

 

[17]

Nucleation-controlled growth

E. coli and S. aureus

ZnCl2

FeCl2·4H2O

Cubic FCC structure

 

[32]

E. coli (DH5α)

Commercial ZnO

Polyethylene Glycol and Polyvinylpyrolidone

ZnO nanofluid

 

[39]

S. aureus KCCM-11335 and E. coli – DH5α

ZnO NPs

Didodecyldimethyl-ammoniumbromide

Flake-like

E. coli > S. aureus and

[40]

In situ solution casting

E. coli and S. aureus

Zn(NO3)2.6H2O

oil palm empty fruit bunches

ZnO dispersed on cellulose matrix

 

[42]

Green method

B subtilis (NCIM 2063), S. aureus (NCIM 2079), E. coli (2065), K. pneumonia (NCIM 2327)

Fe(NO3)3.9H2O

16-nm-sized spherical Fe2O3 with 0.27 nm d value with (104) planes

16 on B. subtilis

[7]

Green

S. aureus, P. aeruginosa,

E. coli and Bacillus subitilis

FeCl3 and Rhus punjabensis

~ 4-nm-sized spherical NPs

10 on P. aeruginosa

[45]

Green

S. aureus and E. coli

Zn(NO3)2.6H2O

Orange fruit peel

Spherical particles that increases as increasing the annealing temperature

E. coli > S. aureus

[50]

Casting

B. subtilis UPMC1175 and Salmonella enterica serovar Choleraesuis

Zn(NO3)2.6H2O

Starch

Spherical and rod-shaped structure

15 on B. subtilis

[53]

Green and chemical method

E. coli ATCC (25922)

Zn(NO3)2.6H2O

spherical crystalline NPs

[54]

Electrospinning

S. aureus (NCIM 2654) and P. aeruginosa (NCIM 5032)

Zn(AC)2.2H2O

Poly (3-hydroxybutyrate-co-3-hydroxyvalerate) and polyethylene oxide

2.04–2.2 μm diameter ZnO reinforced microfibers

2.2–3.1 μm rod

[55, 64]

Hydrothermal method

S. aureus (ATCC strain 29523) and E. coli (ATCC strain 29522)

Zn(AC)2.2H2O

Chitosan and PVA

uniformly distributed ZnO on the surface of the CS/PVA polymer

20 on S. aureus

[56]

Co-precipitation

S. aureus and P. aeruginosa

ZnSO4

Ethylene glycol, gelatin, polyvinyl alcohol, and polyvinylpyrrolidone

ZnO NPs dispersed on capping agent and its hexagonal shape

[57]

Green synthetic strategy

K. pneumoniae (MTCC3384), S. aureus (MTCC87), E. coli (MTCC41), P. mirabilis

Zn(AC)2.2H2O

11-nm-sized semi-crystalline ZnO with 0.19 nm d-spacing value,

18 on P. mirabilis

[58]

Chemical process

E. coli, K. pneumoniae, S.Typhimurium, S. aureus

Zn(NO3)2.6H2O

∼ 0.526 in the c-axis [0001] direction

[59]

Pomegranate peels (punica granatum)

E. coli and S. aureus

Zn(NO3)2.6H2O

50 nm hexagonal bottom-neck nanopencils

21 on S. aureus

[60]

Green synthesis (Anacardiumoccidentale)

E. coli and S. aureus

FeCl3

26–60-nm-sized irregular shape

[62]

  1. AC acetate, SBET specific surface area (m2/g), pV pore volume (cm3/g), Pd pore diameter (nm), d d-spacing (nm), p crystal plane, ZI(mm) zone of inhibition in millimeter, CTMAB cetyltrimethylammonium bromide

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