Table 1 Experimental conditions of the XRD measurements
From: Progress in Iron Oxides Based Nanostructures for Applications in Energy Storage
Temperature (K) | Heating rate (°C min−1) | Atmosphere | Parameter | Time (min) |
|---|---|---|---|---|
293.15–843.15 | 10 | Helium | – | 55 |
843.15–1265.28 (or 1365.28) | 2 | CO/CO2 | Step: 0.01°, 5° min−1 | 215 or 265 |
1265.28 and 1365.28 | 0 | CO/CO2 | Step: 0.01°, 2° min−1 (full scanning), 1° min−1 (scanning of 8 crystal planes) | 240–420 |