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Table 1 Reaction parameters used in synthesis of monodisperse iron oxide NPs

From: Preparation of Monodisperse Iron Oxide Nanoparticles via the Synthesis and Decomposition of Iron Fatty Acid Complexes

Run

Precursora(mmol)

Surfactantb(mmol)

Solventc(mL)

Temperature (°C)

Time (min)

NP diameter (nm)

1

6

9

18

300

60

4.5 ± 0.4

2

6

9

18

290

120

8.1 ± 0.5

3

6

9

18

320

120

10.1 ± 1.0

4

6

18

18

320

150

13.1 ± 0.8

5

6

9

18

360

60

15.3 ± 0.9

6

6

18

18

340

120

20.4 ± 1.1

  1. aPrecursors used: runs 1–5, iron–oleate complex and run 6, iron-linoelate complex
  2. bSurfactant used: runs 1–5, oleic acids and run 6, linoleic acids
  3. cSolvent used: run 1, Oleylacohol; run 2, Benzyl ether; runs 3–4, ODE; run 5, Tri-octylamine; and run 6, 1-eicosane

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