Table 1 Experimental details of organic–inorganic polymer hybrid sol–gel nanocomposites
Experiment | PSMA (g) | γ-APS (ml) | Ti(ipro4) (ml) | Solvent 1,4-dioxane (ml) | 0.1-M HCl in aqueous | Temperature (°C) | Appearance |
---|---|---|---|---|---|---|---|
PS-Ti-a | 0.050 | - | 0.050 | 2 | 0.0012 | 40 | Turbid |
PS-Ti-b | 0.050 | 0.0083 | 0.040 | 2 | 0.0150 | 60 | Transparent |
PS-Ti-c | 0.025 | 0.0083 | 0.0125 | 2 | 0.0140 | 60 | Transparent |
PS-Ti-d | 0.010 | 0.0041 | 0.0050 | 2 | 0.0070 | 90 | Transparent |
PS-Ti-e | 0.005 | 0.0020 | 0.0025 | 2 | 0.0035 | 50 | Translucent |