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Table 4 Advancing (ACA) and receding contact angles (RCA) of water, apparent surface free energy and the specific surface area (SSA)

From: Modified silicas with different structure of grafted methylphenylsiloxane layer

No.

Scheme of modification

Advancing contact angle θ a (deg.)

Receding contact angle θ a (deg.)

Apparent surface free energy γ S (mJ/m2)

SSA (BET)

aCarbon content (CNH). wt %

Carbon content (XPS). wt %

Protocol 1 (modifying mixture portion on tree stages—25/35/40 vol%)

1

L-S

134

130

10

126

8.9

10.5

2

M

121

109

15

118

9.1

11.2

3

S-L

109

94

21

133

7.5

8.9

Protocol 2 1 (modifying mixture portion on tree stages—40/35/25 vol%)

4

S-L

125

118

14

154

9.6

11.2

5

M

131

120

11

139

9.2

10.9

6

L-S

146

136

5

146

9.3

11.0

  1. aCarbon content evaluated using CNH-analysis

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