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Table 1 Analytical data for copolymers

From: Aggregation Control by Multi-stimuli-Responsive Poly(N-vinylamide) Derivatives in Aqueous System

Run

Copolymer

Yield (%)

Unit ratio in copolymer

M n e (×103)

PDIe

1a

1

59c

NVF:MOENVF = 22:78

8.1

3.8

2b

2

42d

NVF:NVFazo:MOENVF = 6:16:78

4.0

4.8

  1. aPolymerization conditions: Solvent = toluene. Conc. = 2 M. Initiator = AIBN. Temp. = 60 °C. Time = 24 h
  2. bPolymer reaction conditions: Solvent = DMF. Conc. = 1 M. Temp. = 80 °C. Time = 10 h
  3. cDiethyl ether-insoluble part
  4. dAcetone-insoluble part
  5. eDetermined by SEC with polystyrene standard in DMF

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