Table 1 Dependence of the main characteristics of products on composition
Sample number | х | Composition | а, А | Crystallite size, А | TC, °С | Mass loss, % | Literature value а, А |
---|---|---|---|---|---|---|---|
1 | 1.3 | Mn1.3Fe1.7О4 | Amorphous | 315 | 11.5 | ||
2 | 1.2 | Mn1.2Fe1.8О4 | Amorphous | 315 | 19.6 | ||
3 | 1.1 | Mn1.1Fe1.9О4 | Amorphous | 305 | 16.4 | ||
4 | 1 | MnFe2О4 | 8.4184 | 48.8 | 320 | 13.4 | 8.51 |
5 | 0.9 | Mn0.9Fe2.1О4 | 8.4148 | 52.3 | 280 | 6.7 | |
6 | 0.8 | Mn0.8Fe2.2О4 | 8.4148 | 60.9 | 315 | 7.2 | |
7 | 0.6 | Mn0.6Fe2.4О4 | 8.4313 | 66.1 | 315 | 5.3 | |
8 | 0.4 | Mn0.4Fe2.6О4 | Amorphous | 320 | 15.4 | ||
9 | 0.2 | Mn0.2Fe2.8О4 | 8.4075 | 66.3 | 580 | 6.2 | |
10 | 0 | Fe3О4 | 8.3750 | 72.3 | 520 | 0 | 8.397 |